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Sep 6. Description of current state Currently, we use a line focus Empyrean diffractometer located in Mikkeli, Laboratory of Green Chemistry. The diffractometer is good for powder diffraction and for thin film sample investigations.
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We restricted the incident beam by masking for trying to make the point focus beam, but the divergence of the collimated beam is large in horizontal plane and is not suitable for micro beam investigations. We have also several special needs, e. Any of these tasks is not possible to do with the current diffractometer. Description of the target state X-ray microdiffraction analysis uses a very small size X-ray beam to carry out highly localized XRD measurements of a very small area.
Essential feature of the X-ray microdiffractometer is the small diameter of the X-ray beam Fig. Incident beam collimators and a high magnification video camera are used to accurately and precisely position the sample area of interest in the X-ray beam see Fig. A two-dimensional detector is used to collect the entire diffraction data while reducing the number of moving axes and associated uncertainty see Fig. The research field of microdiffraction is rapidly growing in materials research and fabrication, because material properties and product yield and reliability are now analyzed from smaller domains.
X-ray microdiffraction can be used for characterization of the samples with structure domains as in magnetic shape memory materials, as well as for samples with high compositional gradients, contaminations, inclusions, mineralogical samples, tiny cross-sections samples, patterned wafers, micro-devices and so on.
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LUT Material Physics requires for investigations of the MSM materials and devices a possibility to study single crystalline samples orientation, crystal structure with twin boundaries and the crystallographic domains variants oriented differently. Suitable diffractometer for such investigations should have X-ray tube with a point focus, three-axes sample stage rotation and x -y table.
The equipment to be purchased forms the basis for the research of our laboratory. The equipment will be used also teaching and exercises.
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It else helps us attract foreign researchers to work in LUT. View full details. Verification of x-ray machines and x-ray study Aug 17, Aug 20, X-ray film pack Oct 18, Oct 20, X-ray film Oct 12, Jan 23, Jan 20, Film x-ray dental Sep 22,